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In the course of teaching in laboratory, I have constantly been feeling the need of concise volume that gives details of organic synthesis and estimations. The book is the outcome of more than 10 years teaching experience of the author. It covers several types of experiments in organic chemistry, done by me, spread overthe syllabi of different Indian and South Asian Universities. This book provides a broad range of solution to the problems of graded difficulties from organic reactions, rearrangements and reagents along with their isolation and synthetic applications. It also meets the basic requirement of students who are entering into industries, and research institutes. The main goal of this book is to build on the foundation of synthesis and estimation. My objective is to solidify the students understanding of the basic concepts of preparation and estimation. The book is intended to meet the need and requirement of UG and PG students. I have fine tuned the difficulties experienced by the students in doing preparation, analysis and estimation. Outstanding feature of this book is the clarity of experimental section. This book will fulfill the requirement for new approaches in experimental skill and solving problems obtained during chemical transformation and estimation. I hope that students and professionals will find this book most useful and essential